The CHF610-0020 Small Sample Pre-heater is a portable desktop instrument designed to preheat two small cylindrical canisters containing samples of a Plutonium Containing Material (PCM) to a temperature similar to that of the thermal block control temperature of a CHF600-0020 Transportable Small Sample Calorimeter.
When a sample is transferred from the pre-heater into the calorimeter it is nominally at the same temperature as the thermal block. The sample introduces less of a disturbance to the system equilibrium and the measurement time is shorter. This results in a faster sample throughput.
The pre-heater consists of a single aluminium sample block with two chambers, each of which is large enough to accept a sample canister measuring 40 mm (1.57 in) in diameter by 80 mm (3.15 in) high. Access is gained to the chambers by removing the plug units located on the top of the block. Electrical pad heaters are installed on two sides of the block and each end of the block is fitted with a Peltier cooler unit and fan. A platinum resistance thermometer is installed in the block to measure the temperature.
A Peltier temperature controller is mounted inside the pre-heater case and is factory configured to ensure that both Peltier units provide continuous cooling to the aluminium block. A Eurotherm 3216 PID temperature controller is connected to the heaters and to the platinum temperature sensor. A temperature set point can be entered into the panel on the front of block and maintains the constant temperature by applying power to the heater in response to the temperature set point.